HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → Methyl 5-acetyl-2-methoxybenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | Methyl 5-acetylsalicylate | HCID 85444 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Methyl 5-acetyl-2-methoxybenzoate | HCID 606426 | — |
Reaction Steps
To a stirred solution of Methyl 2-hydroxy-5-acetylbenzoate (12 g, 61.7 mmol) in DMF (200 ml) was added cesium carbonate (24.15 g, 74.1 mmol) and MeI (9.64 g, 68 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07547802B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-0e8b641389f9488bb658acf20bf5c606 |
| Source note | uspto-grants-2009_06 |