HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-Aminopropyl)-4-methylpiperazine → HCID 68856199, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-Aminopropyl)-4-methylpiperazine | HCID 78328 | — |
| Reactant | (2-{2-[3-(4-Methylpiperazin-1-yl)-propylamino]-pyrimidin-4-yl}-benzo[b]thiophen-6-ylmethyl)-carbamic acid tert-butyl ester | HCID 68859103 | — |
| Reactant | HCID 86625349 | HCID 86625349 | — |
| Product | HCID 68856199 | HCID 68856199 | — |
Reaction Steps
Using the method of (2-{2-[3-(4-methylpiperazin-1-yl)-propylamino]-pyrimidin-4-yl}-benzo[b]thiophen-6-ylmethyl)-carbamic acid tert-butyl ester, the title compound is synthesized from 2-(2,5-dichloropyrimidin-4-yl)benzo[b]thiophene-6-carbonitrile and 1-(3-aminopropyl)-4-methylpiperazine and isolated as a solid. ES+(m/z) 427 (35Cl) and 429 (37Cl) [M+H].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07547691B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-52b202879daa43f79be932fe06bb64c4 |
| Source note | uspto-grants-2009_06 |