2,4,5-Trichloropyrimidine → HCID 86625360, compound

HRID 1986216Notes

Reaction equation

HRID 1986216 reaction equation
[CH3:1][O:2][C:3]([C:5]1[C:13]2[CH:12]=[C:11]([C:14]3[CH:19]=[CH:18][N:17]=[C:16]([Cl:20])[N:15]=3)[S:10][C:9]=2[CH:8]=[CH:7][CH:6]=1)=[O:4].COC(C1C2C=CSC=2C=CC=1)=O.[Cl:34]C1N=C(Cl)C(Cl)=CN=1>>[CH3:1][O:2][C:3]([C:5]1[C:13]2[CH:12]=[C:11]([C:14]3[C:19]([Cl:34])=[CH:18][N:17]=[C:16]([Cl:20])[N:15]=3)[S:10][C:9]=2[CH:8]=[CH:7][CH:6]=1)=[O:4]

Participants

4

Reactant 3

HCID 2372592,4,5-TrichloropyrimidineHCID 13448678Methyl 1-benzothiophene-4-carboxylateHCID 86625361HCID 86625361, compound

Product 1

HCID 86625360HCID 86625360, compound

Procedure

Using the method of 2-(2-chloropyrimidin-4-yl)-benzo[b]thiophene-4-carboxylic acid methyl ester, the title compound is synthesized from benzo[b]thiophene-4-carboxylic acid methyl ester and 2,4,5-trichloropyrimidine and isolated as a solid.

Workup

  1. customisolated as a solid

Sources & evidence

ORD record
ord-d22ede3cebcd448d8ea80f118f454cfb
Source dataset
uspto-grants-2009_06
Patent number
US07547691B2

Reaction notes

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