HRID1986287

反应详情

EQUATION

反应方程式

HRID 1986287 的结构方程式

PROCEDURE

实验过程

Using the method of 2-{5-chloro-2-[3-(4-methylpiperazin-1-yl)-propylamino]-pyrimidin-4-yl}-benzo[b]thiophene-4-carboxylic acid cyclopropylamide tri-hydrochloride, the title compound is synthesized from 2-(5-bromo-2-chloro-pyrimidin-4-yl)-benzo[b]thiophene-4-carboxylic acid methylamide and isolated as a yellow solid. ES+(m/z) 517 (79Br) and 519 (81Br) [M(free base)+H].

WORKUP

后处理

  1. customisolated as a yellow solid