HRID1986314

反应详情

EQUATION

反应方程式

HRID 1986314 的结构方程式

PROCEDURE

实验过程

Using the method of (R)-2-{5-chloro-2-[3-(2-methylpiperazin-1-yl)-propylamino]-pyrimidin-4-yl}-benzo[b]thiophene-4-carboxylic acid methylamide, the title compound is synthesized from 2-(2,5-dichloropyrimidin-4-yl)-benzo[b]thiophene-4-carboxylic acid cyclopropylamide and (R)-4-(2-aminoethyl)-3-methylpiperazine-1-carboxylic acid tert-butyl ester and isolated as a yellow solid. ES+(m/z) 471 (35Cl) and 473 (37Cl) [M+H].

WORKUP

后处理

  1. customisolated as a yellow solid