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HRID1986322

反应详情

EQUATION

反应方程式

HRID 1986322 的结构方程式

REACTANTS

反应物

2
结构：CN1CCC(CCNc2ncc(Cl)c(-c3cc4c(C(N)=O)cccc4s3)n2)CC1.Cl.Cl
HCID68856045

未命名化合物

结构：Cc1cnc(NCCCN2CCNC[C@@H]2C)nc1-c1cc2c(C(=O)NC3CC3)cccc2s1
HCID68908164

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cnc(NCCCN2CCN(C)C[C@@H]2C)nc1-c1cc2c(C(=O)NC3CC3)cccc2s1.Cl.Cl.Cl
HCID68857396

未命名化合物

PROCEDURE

实验过程

Using the method of 2-{5-chloro-2-[2-(1-methylpiperidin-4-yl)-ethylamino]-pyrimidin-4-yl}-benzo[b]thiophene-4-carboxylic acid amide di-hydrochloride, the title compound is synthesized from (S)-2{5-methyl-2-[3-(2-methylpiperazin-1-yl)-propylamino]-pyrimidin-4-yl}-benzo[b]thiophene-4-carboxylic acid cyclopropylamide and isolated as a yellow solid. ES+(m/z) 479 [M(free base)+H].

WORKUP

后处理

  1. customisolated as a yellow solid