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HRID1986324

反应详情

EQUATION

反应方程式

HRID 1986324 的结构方程式

REACTANTS

反应物

2
结构：CN1CCC(CCNc2ncc(Cl)c(-c3cc4c(C(N)=O)cccc4s3)n2)CC1.Cl.Cl
HCID68856045

未命名化合物

结构：CNC(=O)c1cccc2sc(-c3nc(NCCCN4CCN[C@@H](C)C4)ncc3C)cc12
HCID68856782

未命名化合物

PRODUCTS

生成物

1
结构：CNC(=O)c1cccc2sc(-c3nc(NCCCN4CCN(C)[C@@H](C)C4)ncc3C)cc12.Cl.Cl.Cl
HCID68909366

未命名化合物

PROCEDURE

实验过程

Using the method of 2-{5-chloro-2-[2-(1-methylpiperidin-4-yl)-ethylamino]-pyrimidin-4-yl}-benzo[b]thiophene-4-carboxylic acid amide di-hydrochloride, the title compound is synthesized from (S)-2-{5-methyl-2-[3-(3-methylpiperazin-1-yl)-propylamino]-pyrimidin-4-yl}-benzo[b]thiophene-4-carboxylic acid methylamide and isolated as a yellow solid. ES+(m/z) 453 [M(free base)+H].

WORKUP

后处理

  1. customisolated as a yellow solid