HCID 68871013, compound → HCID 68868411, compound

Participants

Reaction Steps

The product of Step 2 (2.9 g, 7.6 mmol) was hydrogenated in methanol (50 mL) in the presense of 5% Pd/C (250 mg) with a balloon of hydrogen overnight. The reaction mixture was filtered through Celite and concentrated to give the title compound (2.1 g, 79%) as a dark orange solid. MS (ES+) m/e 351 [M+H]+.

Provenance & Evidence