Ethylamine → 2-chloro-N-ethyl-5-nitropyridin-4-amine

HRID 1986354Notes

Reaction equation

[Cl:1][C:2]1[CH:7]=[C:6](Cl)[C:5]([N+:9]([O-:11])=[O:10])=[CH:4][N:3]=1.[CH2:12]([NH2:14])[CH3:13]>>[Cl:1][C:2]1[CH:7]=[C:6]([NH:14][CH2:12][CH3:13])[C:5]([N+:9]([O-:11])=[O:10])=[CH:4][N:3]=1

Participants

Reactant 2

HCID 6341Ethylamine

HCID 122757652,4-Dichloro-5-nitropyridine

Product 1

HCID 591770742-chloro-N-ethyl-5-nitropyridin-4-amine

Procedure

The title compound was prepared by the method of Example 1, Step 4 starting from the product of Example 1, Step 3 and ethylamine. MS (ES+) m/e 202 [M+H]+.

Sources & evidence

ORD record: ord-0dd130d9f5fe4c748a9e771248c2076e
Source dataset: uspto-grants-2009_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07547779B2

Reaction notes

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