HCID 68873525, compound → HCID 68873939, compound

Participants

Reaction Steps

The product of Step 3 (3.3 g, 6.6 mmol) was hydrogenated overnight with a balloon of hydrogen gas in MeOH (50 mL) in the presence of 5% Pd/C (300 mg). The reaction mixture was filtered through Celite and concentrated to give the title compound as a dark oil which was used directly in the next step (˜3.1 g, quant.).

Provenance & Evidence