HuagongsheHuagongshe Chemistry Print Report · For research reference only
Anthranilic Acid → 5,10-Dihydro-11H-dibenzo(b,e)(1,4)diazepin-11-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Anthranilic Acid | HCID 227 | — |
| Reactant | 1-Fluoro-2-nitrobenzene | HCID 73895 | — |
| Product | 5,10-Dihydro-11H-dibenzo(b,e)(1,4)diazepin-11-one | HCID 201327 | 30.9% |
Reaction Steps
2-Fluoronitrobenzene (847 g, 6 mmol) and 2-aminobenzoic acid (274 mg, 2.0 mmol) were reacted according to GP7 to give 130 mg of the title compound (160FE15A).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07550454B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-4772290bf93b4490bf2fa269df881946 |
| Source note | uspto-grants-2009_06 |