1-Phenyl-cyclopropylamine → HCID 57722682, compound

HRID 1986870Notes

Reaction equation

HRID 1986870 reaction equation
[C:1]1([C:7]2([NH2:10])[CH2:9][CH2:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.Cl[C:12]1[N:17]=[C:16]([S:18][C:19]#[N:20])[C:15]([N+:21]([O-:23])=[O:22])=[CH:14][N:13]=1>>[N+:21]([C:15]1[C:16]([S:18][C:19]#[N:20])=[N:17][C:12]([NH:10][C:7]2([C:1]3[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=3)[CH2:9][CH2:8]2)=[N:13][CH:14]=1)([O-:23])=[O:22]

Participants

3

Reactant 2

HCID 1945491-Phenyl-cyclopropylamineHCID 210775882-Chloro-5-nitropyrimidin-4-yl thiocyanate

Product 1

HCID 57722682HCID 57722682, compound

Procedure

(5-Nitro-4-thiocyanato-pyrimidin-2-yl)-(1-phenyl-cyclopropyl)-amine was prepared by addition of the above amine to 2-chloro-5-nitro-4-thiocyanato-pyrimidine using the procedure described in Example 17. m/z calcd. C14H10N5O2S [M−H]−: 312.33. Found: 312.10.

Sources & evidence

ORD record
ord-9f5d4185e9944918a60ec25897f3de3e
Source dataset
uspto-grants-2009_06
Patent number
US07550473B2

Reaction notes

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