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Hydrochloric Acid → 1-Phenyl-2-chloro-2-methylpropane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | 2-Methyl-1-phenyl-2-propanol | HCID 7531 | — |
| 生成物 | 1-Phenyl-2-chloro-2-methylpropane | HCID 296357 | — |
反応手順
A mixture of 5.92 g (40 mmoles) of 1-phenyl-2-hydroxy-2-methylpropane and 50 mL conc. hydrochloric acid was stirred at ice bath temperature for 1 h and at RT for 3 h. The reaction mixture was then extracted with ether. The organic layer was dried over MgSO4. Solvent removal gave 1-phenyl-2-chloro-2-methylpropane.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07550489B2 |
| 出典データセット | uspto-grants-2009_06 |
| ORD ID | ord-0cb68b924e0b46afaf29ccde42b50664 |
| 出典メモ | uspto-grants-2009_06 |