Hydrochloric Acid → HCID 22882785, compound

Participants

Reaction Steps

To a solution of (+)-(4aS,7S,8S,8aR)-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol (24 mg, 0.12 mmol) in MeOH (2 mL) was added a solution of methanolic HCl (0.4 mL, prepared from 0.5 mL conc. HCl in 30 mL of MeOH). The solution was stirred for 1 H at ambient temperature and concentrated in vacuo.

Provenance & Evidence