HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86610191, compound → HCID 86610189, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86610191 | HCID 86610191 | — |
| Reactant | HCID 86634648 | HCID 86634648 | — |
| Product | HCID 86610189 | HCID 86610189 | — |
Reaction Steps
Phosphate 12 is prepared similarly to phosphate 5 starting from azide 11 (0.503 g, 2.66 mmol). Coarse purification by column chromatography and silica gel (0.35% ammonia (20% aqueous solution in i-PrOH) pale yellow oil 12 (0.353 g, 46%). Rf 0.4 (i-PrOH/25%-NH4OHaq/H2O 6/4/1). This product is used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07553615B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-bcb9f28c071f47aeb51cbb6facd8abe1 |
| Source note | uspto-grants-2009_06 |