HCID 19608958, compound → HCID 11718232, compound

HRID 1987814Notes

Reaction equation

HRID 1987814 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[CH:8]=[C:7]([C:12](Cl)=[O:13])[CH:6]=[CH:5]2.[S:15]1[C:19]2=[CH:20][CH:21]=[CH:22][C:23]([NH2:24])=[C:18]2[N:17]=[C:16]1[NH2:25]>>[NH2:25][C:16]1[S:15][C:19]2[CH:20]=[CH:21][CH:22]=[C:23]([NH:24][C:12]([C:7]3[CH:6]=[CH:5][C:4]4[C:9](=[CH:10][CH:11]=[C:2]([Br:1])[CH:3]=4)[CH:8]=3)=[O:13])[C:18]=2[N:17]=1

Participants

3

Reactant 2

HCID 19608958HCID 19608958, compoundHCID 218796066-Bromo-2-naphthoyl chloride

Product 1

HCID 11718232HCID 11718232, compound

Procedure

This material was prepared analogous to the procedure described for Example 1(b). 6-Bromo-naphthalene-2-carbonyl chloride, Example 1(a), (127 mg, 0.47 mmol) reacted with benzothiazole-2,4-diamine (77 mg, 0.47 mmol, prepared according to the procedure described in WO03099284) to give the title compound as an amorphous solid. MS (ESI, pos. ion.) m/z: 400 (M+1).

Workup

  1. customThis material was prepared analogous to the procedure
  2. customprepared

Sources & evidence

ORD record
ord-a29c19b455d040a6b482eaa1526891f8
Source dataset
uspto-grants-2009_06
Patent number
US07553848B2

Reaction notes

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