6-Bromo-2-naphthoyl chloride → HCID 178521821, compound

HRID 1987816Notes

Reaction equation

HRID 1987816 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[CH:8]=[C:7]([C:12](Cl)=[O:13])[CH:6]=[CH:5]2.[NH:15]1[C:19]2[CH:20]=[CH:21][C:22]([NH2:24])=[CH:23][C:18]=2[N:17]=[CH:16]1>>[NH:15]1[C:19]2[CH:20]=[CH:21][C:22]([NH:24][C:12]([C:7]3[CH:6]=[CH:5][C:4]4[C:9](=[CH:10][CH:11]=[C:2]([Br:1])[CH:3]=4)[CH:8]=3)=[O:13])=[CH:23][C:18]=2[N:17]=[CH:16]1

Participants

3

Reactant 2

HCID 218796066-Bromo-2-naphthoyl chlorideHCID 178507353HCID 178507353, compound

Product 1

HCID 178521821HCID 178521821, compound

Procedure

This material was prepared analogous to the procedure described for Example 1 (b). 6-Bromo-naphthalene-2-carbonyl chloride, Example 1(a), reacted with 1H-benzoimidazol-5-ylamine (TimTec) to give the title compound as an amorphous solid. MS (ESI, pos. ion.) m/z: 366 (M+1).

Workup

  1. customThis material was prepared analogous to the procedure

Sources & evidence

ORD record
ord-50f4a76b35d54c17ba67c92dcef22690
Source dataset
uspto-grants-2009_06
Patent number
US07553848B2

Reaction notes

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