HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tyr(3-tBu)-OMe → Tyr(3-tBu)-NHMe
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tyr(3-tBu)-OMe | HCID 15549498 | — |
| Reactant | Monomethylamine methanol | HCID 57454252 | — |
| Product | Tyr(3-tBu)-NHMe | HCID 131722741 | — |
Reaction Steps
A mixture of Tyr(3-tBu)-OMe (12 g, 48 mmol) and a 40% methylamine methanol solution (80 ml) was stirred at room temperature for 14 hours. The reaction mixture was concentrated under reduced pressure, giving Tyr(3-tBu)-NHMe (T2) (12 g) as a crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07553969B1 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-773156ddadfc4fc1b0e9b683e50ae329 |
| Source note | uspto-grants-2009_06 |