HRID1988356

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID10796

Cesium carbonate

CCs2O3

HCID97053

Glycine, N-methyl-N-[(phenylmethoxy)carbonyl]-

C11H13NO4

结构：CC(C)(C)c1cc(C(=O)CBr)cc(C(C)(C)C)c1O

HCID616161

2-Bromo-1-(3,5-di-tert-butyl-4-hydroxyphenyl)ethan-1-one

C16H23BrO2

PRODUCTS

生成物

结构：CN(CC(=O)OCC(=O)c1cc(C(C)(C)C)c(O)c(C(C)(C)C)c1)C(=O)OCc1ccccc1

HCID22987727

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

This intermediate is obtained in a standard fashion starting from Cbz-Sarcosine and 1-[3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl]-2-bromo-ethanone in the presence of caesium carbonate in DMF.

WORKUP

后处理

customThis intermediate is obtained in a standard fashion