HRID1988410

反应详情

EQUATION

反应方程式

HRID 1988410 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of 1-[2-(3-Nitro-phenyl)-ethyl]-piperidine in ethanol was added a catalytic amount 10% activated palladium on carbon and excess hydrogen gas. This mixture was allowed to stir overnight, then filtered and concentrated. The product was clean enough for the next reaction. 60% yield. MH+=205.1.

WORKUP

后处理

  1. filtrationfiltered
  2. concentrationconcentrated
  3. customThe product was clean enough for the next reaction