Bromomethyl methyl ether → HCID 68704770, compound

HRID 1988843Notes

Reaction equation

HRID 1988843 reaction equation
[Cl:1][C:2]1[CH:20]=[C:19]([Cl:21])[CH:18]=[CH:17][C:3]=1[CH2:4][O:5][C:6]1[CH:11]=[CH:10][N:9]=[C:8]2[C:12]([CH3:16])=[C:13]([CH3:15])[NH:14][C:7]=12.[CH3:22][O:23][CH2:24]Br>>[ClH:1].[Cl:1][C:2]1[CH:20]=[C:19]([Cl:21])[CH:18]=[CH:17][C:3]=1[CH2:4][O:5][C:6]1[CH:11]=[CH:10][N:9]=[C:8]2[C:12]([CH3:16])=[C:13]([CH3:15])[N:14]([CH2:22][O:23][CH3:24])[C:7]=12

Participants

3

Reactant 2

HCID 83093Bromomethyl methyl etherHCID 68702597HCID 68702597, compound

Product 1

HCID 68704770HCID 68704770, compoundYield 58.9%

Procedure

In accordance with the same procedures as in Step 2 of Example 33, except for using 7-(2,4-dichlorobenzyloxy)-2,3-dimethyl-1H-pyrrolo[3,2-b]pyridine prepared in Step 2 and bromomethyl methyl ether, the titled compound was obtained as a white solid. (Yield: 58.9%)

Sources & evidence

ORD record
ord-0db3d8682e454b15b0fe6bc4d87f1ba1
Source dataset
uspto-grants-2010_01
Patent number
US07642269B2

Reaction notes

Loading…