HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Difluorobenzyl alcohol → 4-[(3,5-Difluorophenyl)methoxy]-3-nitropyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Difluorobenzyl alcohol | HCID 522721 | — |
| Reactant | 4-Chloro-3-nitropyridine | HCID 2735781 | — |
| Product | 4-[(3,5-Difluorophenyl)methoxy]-3-nitropyridine | HCID 68704860 | 78% |
Reaction Steps
In accordance with the same procedures as in Preparation 2, except for using 4-chloro-3-nitropyridine prepared in Step 1 of Preparation 1 and 3,5-difluorobenzyl alcohol, the titled compound was obtained as a yellow solid. (Yield: 78.0%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07642269B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-69c17bbef72140f6ad636df971a3b42f |
| Source note | uspto-grants-2010_01 |