3-Pyridinemethanol → HCID 68702817, compound

HRID 1988849Notes

Reaction equation

HRID 1988849 reaction equation
Cl[C:2]1[CH:7]=[CH:6][N:5]=[CH:4][C:3]=1[N+:8]([O-:10])=[O:9].[N:11]1[CH:16]=[CH:15][CH:14]=[C:13]([CH2:17][OH:18])[CH:12]=1>>[N:11]1[CH:16]=[CH:15][CH:14]=[C:13]([CH2:17][O:18][C:2]2[CH:7]=[CH:6][N:5]=[CH:4][C:3]=2[N+:8]([O-:10])=[O:9])[CH:12]=1

Participants

3

Reactant 2

HCID 75103-PyridinemethanolHCID 27357814-Chloro-3-nitropyridine

Product 1

HCID 68702817HCID 68702817, compoundYield 78.5%

Procedure

In accordance with the same procedures as in Preparation 2, except for using 4-chloro-3-nitropyridine prepared in Step 1 of Preparation 1 and 3-pyridyl carbinol, the titled compound was obtained as a yellow solid. (Yield: 78.5%)

Workup

  1. customIn accordance with the same procedures as in Preparation 2

Sources & evidence

ORD record
ord-cf41a30d3a4e490d94a386cd84d0e9b3
Source dataset
uspto-grants-2010_01
Patent number
US07642269B2

Reaction notes

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