4-(4-Methylpiperazino)-1,2-benzenediamine → HCID 135820279, compound

HRID 1988976Notes

Reaction equation

HRID 1988976 reaction equation
[N+:1]([C:4]1[CH:5]=[CH:6][C:7]([O:10][C:11]2[CH:19]=[CH:18][CH:17]=[C:16]3[C:12]=2[C:13]([CH:20]=O)=[N:14][NH:15]3)=[N:8][CH:9]=1)([O-:3])=[O:2].[CH3:22][N:23]1[CH2:28][CH2:27][N:26]([C:29]2[CH:30]=[C:31]([NH2:36])[C:32]([NH2:35])=[CH:33][CH:34]=2)[CH2:25][CH2:24]1>>[CH3:22][N:23]1[CH2:24][CH2:25][N:26]([C:29]2[CH:34]=[CH:33][C:32]3[N:35]=[C:20]([C:13]4[C:12]5[C:16](=[CH:17][CH:18]=[CH:19][C:11]=5[O:10][C:7]5[CH:6]=[CH:5][C:4]([N+:1]([O-:3])=[O:2])=[CH:9][N:8]=5)[NH:15][N:14]=4)[NH:36][C:31]=3[CH:30]=2)[CH2:27][CH2:28]1

Participants

3

Reactant 2

HCID 27635454-(4-Methylpiperazino)-1,2-benzenediamineHCID 178520031HCID 178520031, compound

Product 1

HCID 135820279HCID 135820279, compound

Procedure

The formation of the tide compound is carried out using 4-(5-nitropyridin-2-yloxy)-1H-indazole-3-carbaldehyde and 4-(4-methylpiperazin-1-yl)-benzene-1,2-diamine using the method described above in Example 4.

Sources & evidence

ORD record
ord-e135b41aad1945278951f4a97138a801
Source dataset
uspto-grants-2010_01
Patent number
US07642278B2

Reaction notes

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