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HRID1989316

反应详情

EQUATION

反应方程式

HRID 1989316 的结构方程式

REACTANTS

反应物

2
结构：CC1(C)OB(c2cccnc2)OC1(C)C
HCID2734656

3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine

C11H16BNO2

结构：Clc1ccc(-c2cc(C3CC3)nc(-n3cnc(Br)c3)n2)cc1
HCID57468738

未命名化合物

PRODUCTS

生成物

1
结构：Clc1ccc(-c2cc(C3CC3)nc(-n3cnc(-c4cccnc4)c3)n2)cc1
HCID57468864

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 2-(4-bromo-imidazol-1-yl)-4-(4-chloro-phenyl)-6-cyclopropyl-pyrimidine (example E.14) (0.15 g, 0.4 mmol) and commercially available 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine (0.08 g, 0.4 mmol) according to the general procedure VI. Obtained as an off-white solid (0.015 g, 10%). MS (ISP) 374.0 [(M+H)+]; mp 180-182° C.