HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromobenzene-1-sulfonamide → HCID 57469022, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromobenzene-1-sulfonamide | HCID 2734765 | — |
| Reactant | HCID 60209342 | HCID 60209342 | — |
| Product | HCID 57469022 | HCID 57469022 | — |
Reaction Steps
The title compound was prepared from 3-[4-methyl-6-(4-trifluoromethyl-phenyl)pyridin-2-yl]-benzeneboronic acid (example G.10) (0.407 g, 1.14 mmol) and commercially available 3-bromobenzenesulfonamide (177 mg, 1.14 mmol) according to the general procedure VI. Obtained as a white solid (0.052 g, 10%). MS (ISP) 469.4 [(M+H)+]; mp 200° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07642264B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-1422b3a6ced848d489475f18b852019b |
| Source note | uspto-grants-2010_01 |