HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(tert-Butylaminosulphonyl)benzeneboronic acid → HCID 68693830, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(tert-Butylaminosulphonyl)benzeneboronic acid | HCID 44119538 | — |
| Reactant | HCID 86615445 | HCID 86615445 | — |
| Product | HCID 68693830 | HCID 68693830 | — |
Reaction Steps
The title compound was prepared from 2′-chloro-4-methyl-6-(4-trifluoromethylphenyl)-[2,4′]bipyridinyl (example E.94) (0.350 g, 1.0 mmol) and commercially available 3-(tert-butylsulfamoyl)-benzeneboronic acid (0.283 g, 1.1 mmol) according to the general procedure VI. Obtained as a white solid (0.426 g, 81%). MS (ISP) 526.2 [(M+H)+]; mp 189° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07642264B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-f55dcfbdb5dd4011a9dcbb3b80d87cb0 |
| Source note | uspto-grants-2010_01 |