HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-tert-butyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)thiophene-2-sulfonamide → HCID 86615463, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-tert-butyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)thiophene-2-sulfonamide | HCID 57468817 | — |
| Reactant | HCID 86615464 | HCID 86615464 | — |
| Product | HCID 86615463 | HCID 86615463 | — |
Reaction Steps
The title compound was prepared from 2′-iodo-4-trifluoromethyl-6-(4-trifluoromethylphenyl)-[2,4′]bipyridinyl (example E.98) (0.494 g, 1.0 mmol) and N-tert-butyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-thiophene-2-sulfonamide (example F.1) (0.380 g, 1.1 mmol) according to the general procedure VI. Obtained as a white solid (0.360 g, 62%). MS (ISP) 586.2 [(M+H)+]; mp 220° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07642264B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-006aea14ce93425c9fa45b3c23e2d17c |
| Source note | uspto-grants-2010_01 |