HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Aminosulphonyl)benzeneboronic acid → HCID 24759874, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Aminosulphonyl)benzeneboronic acid | HCID 22391977 | — |
| Reactant | 2-Chloro-4-[6-methyl-4-(4-trifluoromethylphenyl)-pyridin-2-yl]-pyrimidine | HCID 57468797 | — |
| Product | HCID 24759874 | HCID 24759874 | — |
Reaction Steps
The title compound was prepared from 2-chloro-4-[6-methyl-4-(4-trifluoromethylphenyl)-pyridin-2-yl]-pyrimidine (example E.83) (0.150 g, 0.381 mmol) and commercially available (4-aminosulfonylphenyl)boronic acid [CAS-No. 613660-87-0] (0.130 g, 0.457 mmol) according to the general procedure VI. Obtained as a white solid (0.045 g, 25%). MS (ISP) 471.1 [(M+H)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07642264B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-956d441b6ddf4274a4d52a12a0bab6a0 |
| Source note | uspto-grants-2010_01 |