HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichloroethane → 1,1'-[ethane-1,2-diylbis(oxy)]bis(4-methylbenzene)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichloroethane | HCID 11 | — |
| Reactant | M-Cresol | HCID 342 | — |
| Reactant | P-Cresol | HCID 2879 | — |
| Reactant | 1,2-Dibromoethane | HCID 7839 | — |
| Solvent | 1,1'-[Ethane-1,2-diylbis(oxy)]bis(3-methylbenzene) | HCID 97354 | — |
| Product | 1,1'-[ethane-1,2-diylbis(oxy)]bis(4-methylbenzene) | HCID 278437 | — |
| Product | HCID 21844701 | HCID 21844701 | — |
Reaction Steps
A method in which 4-methylphenol is incorporated into, or added to, 3-methylphenol that is a main raw material for synthesis of 1,2-bis(3-methylphenoxy)ethane, such that an amount corresponding to the content defined in the present invention is attained, and the resultant mixture is reacted with 1,2-dihalogenoethane such as 1,2-dibromoethane or 1,2-dichloroethane, or the like. In this manner, 1-(3-methylphenoxy)-2-(4-methylphenoxy)ethane and/or 1,2-bis(4-methylphenoxy)ethane are/is formed in 1,2-bis(3-methylphenoxy)ethane that is a main product, to obtain a composition having a desired content thereof. According to this method, the composition of the present invention can be prepared directly, in the course of synthesis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07645396B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-deaec1fff860482f8c79ad672630314f |
| Source note | uspto-grants-2010_01 |