HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 4-chlorosulfonyl-2-methylphenoxyacetate → Ethyl [4-(chlorosulfonyl)-2,5-dimethylphenoxy]acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 4-chlorosulfonyl-2-methylphenoxyacetate | HCID 11415129 | — |
| Reactant | Ethyl 2,5-dimethylphenoxyacetate | HCID 17065224 | — |
| Product | Ethyl [4-(chlorosulfonyl)-2,5-dimethylphenoxy]acetate | HCID 20768123 | — |
Reaction Steps
The title compound was prepared according to the method described for preparing compound 10.2, using compound 21.1 as the starting material. 1H NMR (400 MHz) (CDCl3) δ 7.86 (1H, s); 6.61 (1H, s); 4.74 (2H, s); 4.30 (2H, q, J=7.1 Hz); 2.71 (3H, s); 2.31 (3H, s); 1.32 (3H, t, J=7.1 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07645779B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-ae57dfd4bcc84e439999c26ded2a67fc |
| Source note | uspto-grants-2010_01 |