HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-3-methylbenzaldehyde → 4-[(4-Formyl-2-methylphenyl)sulfanyl]-2,5-dimethylphenoxy-acetic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-3-methylbenzaldehyde | HCID 2757659 | — |
| Reactant | 2,5-Dimethyl-4-mercaptophenoxy-acetic acid ethyl ester | HCID 20768107 | — |
| Reactant | 4-[(4-Formylphenyl)sulfanyl]-2-methylphenoxy-acetic acid ethyl ester | HCID 20768121 | — |
| Product | 4-[(4-Formyl-2-methylphenyl)sulfanyl]-2,5-dimethylphenoxy-acetic acid ethyl ester | HCID 20768120 | — |
Reaction Steps
The title compound was prepared according to the method described for preparing compound 7.1, using compound 21.3 and 4-chloro-3-methylbenzaldehyde as the starting materials. 1H NMR (400 MHz) (CDCl3) δ 9.86 (1H, s); 7.62 (1H, s); 7.44 (1H, d, J=8.1 Hz); 7.33 (1H, s); 6.70 (1H, s); 6.62 (1H, d, J=8.1 Hz); 4.68 (2H, s); 4.29 (2H, q, J=7.1 Hz); 2.46 (3H, s); 2.29 (3H, s); 2.26 (3H, s); 1.32 (3H, t, J=7.1 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07645779B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-b3ac26b625ad463da045720ec487aa2c |
| Source note | uspto-grants-2010_01 |