4-Bromobutyryl chloride → HCID 59128820, compound

HRID 1991380Notes

Reaction equation

HRID 1991380 reaction equation
[C:1]([C:5]1[CH:22]=[CH:21][CH:20]=[CH:19][C:6]=1[O:7][C:8]1[C:13]([NH:14][C:15](=[S:18])[NH:16][NH2:17])=[CH:12][CH:11]=[CH:10][N:9]=1)([CH3:4])([CH3:3])[CH3:2].[Br:23][CH2:24][CH2:25][CH2:26][C:27](Cl)=O>>[Br:23][CH2:24][CH2:25][CH2:26][C:27]1[S:18][C:15]([NH:14][C:13]2[C:8]([O:7][C:6]3[CH:19]=[CH:20][CH:21]=[CH:22][C:5]=3[C:1]([CH3:4])([CH3:2])[CH3:3])=[N:9][CH:10]=[CH:11][CH:12]=2)=[N:16][N:17]=1

Participants

3

Reactant 2

HCID 702254-Bromobutyryl chlorideHCID 59128834HCID 59128834, compound

Product 1

HCID 59128820HCID 59128820, compound

Procedure

Example 102a was synthetized following the procedure for Example 1 using 4-(2-(2-tert-butylphenoxy)pyridin-3-yl)thiosemicarbazide (Example 1b) with 4-bromobutanoyl chloride.

Sources & evidence

ORD record
ord-83b19f64a0814c9599d410cb94d5b47b
Source dataset
uspto-grants-2010_01
Patent number
US07645778B2

Reaction notes

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