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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1992323Generated: October 31, 2026

HCID 67348061, compound → HCID 11589857, compound

https://huagongshe.com/reaction/1992323

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67348061HCID 67348061—
ReactantHCID 86642355HCID 86642355—
CatalystCopper(1+) iodide; Copper(I) iodide; Cuprous iodide; Cuprous iodide (CuI)HCID 24350—
CatalystHCID 178418476HCID 178418476—
SolventDimethylformamideHCID 6228—
ProductHCID 11589857HCID 11589857—

Reaction Conditions

Temperature85 °C

Reaction Steps

The title compound was prepared by the general method described by Nishihara et al., J. Org. Chem., 2000, 65, 1780-1787. To a solution of 2-(methylthio)-5-[(trimethylsilyl)ethynyl]pyrimidine (0.55 g, 2.47 mmol) and 1-{[(4-methyl-2,5-dioxoimidazolidin-4-yl)methyl]sulfonyl}-1,2,3,6-tetrahydropyridin-4-yl trifluoromethanesulfonate (0.94 g, 2.22 mmol) in DMF (5 mL) was added CuI (10 mol %) and PdCl2(PPh3)2 (5 mol %) and the mixture was heated at 85° C. for 6 hours. The mixture was partitioned between EtOAc (20 mL) and water (10 mL), and the aqueous layer was extracted three times with EtOAc. The combined organic layers were washed with brine, water and concentrated to a brown oil (1.6 g). The title compound was obtained as a solid (10 mg) following purification by preparative HPLC (using a Xterra-Prep-MS-C18 (50×19) column with a 12 minutes gradient 5-35% of acetonitrile in water with 0.06% NH3).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07648992B2
Source datasetuspto-grants-2010_01
ORD IDord-83f92b84256b4270843774339086b0a5
Source noteuspto-grants-2010_01