HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → Methyltriphenylphosphonium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | Methyltriphenylphosphonium iodide | HCID 638159 | — |
Reaction Steps
To a solution of triphenylphosphine (30 g, 0.114 mol) in benzene (200 mL) was added methyl iodide (11 ml, 0.1756 mol) dropwise, and the solution stirred at room temperature for 15 min under a nitrogen atmosphere. The sub-title compound formed as a colourless solid, which was filtered and then dried. Yield: 30 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07648985B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-c161c8bf79d24b868d2951a26bd2e579 |
| Source note | uspto-grants-2010_01 |