HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86087074, compound → HCID 86087076, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86087074 | HCID 86087074 | — |
| Reactant | HCID 178491912 | HCID 178491912 | — |
| Product | HCID 86087076 | HCID 86087076 | — |
Reaction Steps
Synthesized according to the procedure utilized for Example 46 (Step 2) using 2-methyl-4,4-bis(methyloxy)-3-[4-(methyloxy)phenyl]-2-cyclobuten-1-one (260) and 4-methoxyphenylmagnesium bromide. 1H NMR (CDCl3, 300 MHz) δ 7.39-7.29 (m, 4H), 7.10-6.88 (m, 4H), 3.88 (s, 3H), 3.85 (s, 3H), 2.47 (s, 3H). TLC (60:40; hexanes/EtOAc): Rf=0.23.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07649093B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-94e8842566ef46b6a66aa86a39765c0b |
| Source note | uspto-grants-2010_01 |