Barium pentafluorobenzenesulphonate → Calcium pentafluorobenzenesulfonate

HRID 1993135노트

반응식

HRID 1993135 반응식
[F:1][C:2]1[C:7]([S:8]([OH:11])(=[O:10])=[O:9])=[C:6]([F:12])[C:5]([F:13])=[C:4]([F:14])[C:3]=1[F:15].[OH-].[Ca+2:17].[OH-]>>[F:1][C:2]1[C:7]([S:8]([O-:11])(=[O:10])=[O:9])=[C:6]([F:12])[C:5]([F:13])=[C:4]([F:14])[C:3]=1[F:15].[Ca+2:17].[F:1][C:2]1[C:7]([S:8]([O-:11])(=[O:10])=[O:9])=[C:6]([F:12])[C:5]([F:13])=[C:4]([F:14])[C:3]=1[F:15]

참가 물질

3

반응물 2

HCID 417247Barium pentafluorobenzenesulphonateHCID 6093208Calcium Hydroxide

생성물 1

HCID 10075793Calcium pentafluorobenzenesulfonate

실험 절차

To 1000 g of 5% pentafluorobenzene sulfonic acid aqueous solution stirred at room temperature, 30 g of calcium hydroxide was added. The stirring was continued while measuring the pH value. At the time when the pH value reached 6, approximately, filtration was done by using a 0.4 μm glass filter to remove the insoluble components, so as to obtain a calcium pentafluorobenzenesulfonate aqueous solution.

후처리

  1. filtrationapproximately, filtration
  2. filtrationfilter
  3. customto remove the insoluble components

출처 및 근거

ORD 기록
ord-9521e331b91a4f3da6108c57e6673596
출처 데이터셋
uspto-grants-2010_01
특허 번호
US07651639B2

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