HuagongsheHuagongshe Chemistry Print Report · For research reference only
Borane;tetrahydrofuran → HCID 23155228, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Borane;tetrahydrofuran | HCID 2723981 | — |
| Reactant | HCID 59596342 | HCID 59596342 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 23155228 | HCID 23155228 | — |
Reaction Steps
3-Amino-N,N-dimethyl-5-trifluoromethyl-benzamide (2.0 g; 8.6 mmol) dissolved in THF (20 ml) is reduced with a 1 M solution of BH3.THF (26 ml) as described in Stage 134.1, yielding the title compound: MS: [M+1]+=219.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07652022B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-ee3663fa87894d688ece044822727223 |
| Source note | uspto-grants-2010_01 |