Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methyl-1,3-benzothiazol-5-ol → 2-methyl-5-benzothiazolyl 2,3,4-tri-O-acetyl-5-thio-beta-D-xylopyranoside
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methyl-1,3-benzothiazol-5-ol | HCID 699799 | — |
| 반응물 | 2,3,4-Tri-o-acetyl-5-thioxylopyranosyl bromide | HCID 11382683 | — |
| 생성물 | 2-methyl-5-benzothiazolyl 2,3,4-tri-O-acetyl-5-thio-beta-D-xylopyranoside | HCID 68538140 | 6% |
반응 단계
By carrying out the process in a manner similar to example 7, starting from 2,3,4-tri-O-acetyl-5-thio-D-xylopyranosyl bromide and 2-methyl-5-hydroxybenzothiazole, the desired product is obtained in the form of white crystals with a yield of 6%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07652032B2 |
| 출처 데이터셋 | uspto-grants-2010_01 |
| ORD ID | ord-e8a30dd8fc7440608e7682ea3b084b83 |
| 출처 메모 | uspto-grants-2010_01 |