HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3,4-Tri-o-acetyl-5-thioxylopyranosyl bromide → HCID 68897997, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3,4-Tri-o-acetyl-5-thioxylopyranosyl bromide | HCID 11382683 | — |
| Reactant | HCID 178429808 | HCID 178429808 | — |
| Product | HCID 68897997 | HCID 68897997 | 38% |
Reaction Steps
By carrying out the process in a manner similar to example 7, starting from 2,3,4-tri-O-acetyl-5-thio-D-xylopyranosyl bromide and 2-methyl-7-hydroxyimidazo[1,2-α]-pyridine obtained according to preparation 3, the desired product is obtained in the form of a white solid with a yield of 38%. The product obtained is used directly in the deacetylation step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07652032B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-0d6c63c5f3c347a5a200404d82ace990 |
| Source note | uspto-grants-2010_01 |