HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3,4-Tri-o-acetyl-5-thioxylopyranosyl bromide → 2-methylimidazo[1,2-alpha]pyridin-6-yl 2,3,4-tri-O-acetyl-5-thio-beta-D-xylopyranoside
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3,4-Tri-o-acetyl-5-thioxylopyranosyl bromide | HCID 11382683 | — |
| Reactant | HCID 67352409 | HCID 67352409 | — |
| Product | 2-methylimidazo[1,2-alpha]pyridin-6-yl 2,3,4-tri-O-acetyl-5-thio-beta-D-xylopyranoside | HCID 68898009 | 13% |
Reaction Steps
By carrying out the process in a manner similar to example 7, starting from 2,3,4-tri-O-acetyl-5-thio-D-xylopyranosyl bromide and 2-methyl-6-hydroxyimidazo[1,2-α]pyridine obtained according to preparation 5, the desired product is obtained in the form of a white solid with a yield of 13%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07652032B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-b12e5b38d40e46d7a7ec4d615573ec30 |
| Source note | uspto-grants-2010_01 |