O-Phenylenediamine → HCID 599710, compound

HRID 1993790Notes

Reaction equation

HRID 1993790 reaction equation
[C:1]1([NH2:8])[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[NH2:7].O=[C:10]([CH2:16][CH2:17][C:18](OCC)=[O:19])[C:11]([O:13][CH2:14][CH3:15])=[O:12]>>[O:19]=[C:18]1[NH:8][C:1]2[C:2](=[CH:3][CH:4]=[CH:5][CH:6]=2)[N:7]=[C:17]1[CH2:16][CH2:10][C:11]([O:13][CH2:14][CH3:15])=[O:12]

Participants

3

Reactant 2

HCID 7243O-PhenylenediamineHCID 80070Diethyl alpha-ketoglutarate

Product 1

HCID 599710HCID 599710, compoundYield 72%

Procedure

The title compound was prepared from 1,2-phenylenediamine and diethyl 2-oxopentanedioate using methods as described in the literature for similar compounds (Weygand et al., 1962) in 72% yield.

Sources & evidence

ORD record
ord-a891b1c4c3e34b5ebd919d65bfc69703
Source dataset
uspto-grants-2010_01
Patent number
US07652036B2

Reaction notes

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