HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178422553, compound → HCID 178422554, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178422553 | HCID 178422553 | — |
| Solvent | Cyclohexane | HCID 8078 | — |
| Product | HCID 178422554 | HCID 178422554 | — |
Reaction Steps
This compound was isolated as the second and more polar product in the preparation of cis-2-(1-{4-[(5-fluoro-indan-2-ylmethyl)-amino]-cyclohexyl}-5-methyl-1H-benzoimidazol-2-yl)-propan-2-ol. The analysis of the 1H-NMR confirmed the trans-conformation of the cyclohexane. LC-MS showed a single peak, C27H34FN3O (m/e) calcd 435.2686, obsd 436.3 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07652053B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-d47487b24c704688930cc38cce513f06 |
| Source note | uspto-grants-2010_01 |