Sodium Hydroxide → HCID 86620050, compound

Participants

Reaction Conditions

Reaction Steps

The intermediate from step G (3.98 g, 5.31 mmol) was dissolved in 100 mL of MeOH and was added 0.1 mL of 2N NaOH. The mixture was heated to 45° C. for 1 hr. Volatiles were removed in vacuo. The crude residue was purified on silica gel and eluted a combination of EtOAc/hexanes (10-30% EtOAc/hexanes linear gradient). This provided the title compound. MS: (MH)+601

Provenance & Evidence