HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → 4-(Pyridin-3-yloxy)benzohydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | Methyl 4-(pyridin-3-yloxy)benzoate | HCID 47002921 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-(Pyridin-3-yloxy)benzohydrazide | HCID 59135434 | 100% |
Reaction Steps
Methyl 4-(pyridine-3-yloxy)benzoate (4.8 g, 20.94 mmol) was dissolved in ca. 150 mL of EtOH and anhydrous hydrazine (4.08 g, 4.0 mL) was added via a syringe. The resulting yellow solution was refluxed for 24 hrs. Then solvent was removed in vacuo to give the title product (4.8 g, 100% yield) as yellow viscous oil, which upon standing slowly solidified.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07652051B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-074541bde4fc4d1fadd3558c8c7c251a |
| Source note | uspto-grants-2010_01 |