HCID 68684502, compound → HCID 68681761, compound

Participants

Reaction Steps

The alkene from Step 2 (0.755 g, 1.80 mmol) was suspended in MeOH. To this suspension was added Pd/C (10 wt %). The reaction was placed under an atmosphere of hydrogen gas and allowed to stir at rt for 3 h. The mixture was filtered through Celite and concentrated. The residue was purified by column chromatography to give the desired product (0.546 g, 72%). LCMS: (FA) ES+ 392.0 (M+1), ES− 390.0 (M−1).

Provenance & Evidence