3-tert-Butylaniline → HCID 58674698, compound

HRID 1994161Notes

Reaction equation

HRID 1994161 reaction equation
[Si:1]([O:8][CH2:9]/[C:10](=[CH:14]\C1C=CC=C(OC)C=1)/[C:11](O)=[O:12])([C:4]([CH3:7])([CH3:6])[CH3:5])([CH3:3])[CH3:2].[C:23]([C:27]1[CH:28]=[C:29]([CH:31]=[CH:32][CH:33]=1)[NH2:30])([CH3:26])([CH3:25])[CH3:24]>>[Si:1]([O:8][CH2:9][C:10](=[CH2:14])[C:11]([NH:30][C:29]1[CH:31]=[CH:32][CH:33]=[C:27]([C:23]([CH3:26])([CH3:24])[CH3:25])[CH:28]=1)=[O:12])([C:4]([CH3:7])([CH3:6])[CH3:5])([CH3:2])[CH3:3]

Participants

3

Reactant 2

HCID 793343-tert-ButylanilineHCID 68683004HCID 68683004, compound

Product 1

HCID 58674698HCID 58674698, compound

Procedure

The title compound was prepared as described in Example 10, Step 3, using (E)-2-((tert-butyldimethylsilyloxy)methyl)-3-(3-methoxyphenyl)acrylic acid and 3-tert-butyl aniline. LCMS, FA: Rt=2.51 min, [MH+ 348.0].

Sources & evidence

ORD record
ord-7377d55a4c3248ef906d83fc621efdae
Source dataset
uspto-grants-2010_01
Patent number
US07652041B2

Reaction notes

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