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HRID1994221

反应详情

EQUATION

反应方程式

HRID 1994221 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)C(O)(c1ccc(F)cc1)c1ccc(F)cc1
HCID12068840

未命名化合物

结构：CN1[C@@H]2CC=C[C@@]1(O)CC2
HCID53629842

未命名化合物

PRODUCTS

生成物

1
结构：CN1[C@@H]2CC=C[C@@]1(OC(=O)C(O)(c1ccc(F)cc1)c1ccc(F)cc1)CC2
HCID86585677

未命名化合物

PROCEDURE

实验过程

4.5 is prepared analogously to the method according to II.1. Yield: 8.71 g (69% of theory) starting from 8.35 g (0.03 mol) of 3c and 4.18 g (0.03 mol) of tropenol; TLC: Rf value: 0.34 (eluant as in step II.1); melting point: 167° C.-169° C.

WORKUP

后处理

  1. custom4.5 is prepared analogously to the method