HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromopropylate → HCID 86761045, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromopropylate | HCID 28936 | — |
| Reactant | Tropenol | HCID 53629842 | — |
| Product | HCID 86761045 | HCID 86761045 | — |
Reaction Steps
4.9 is prepared analogously to the method according to II.1. Yield: 2.36 g (19% of theory) starting from 9.9 g (0.023 mol) of commercially obtainable isopropyl 4,4′-dibromobenzilate and 3.21 g (0.023 mol) of tropenol; to purify it, the hydrochloride was precipitated and recrystallized from acetonitrile. TLC: Rf value: 0.30 (eluant as in step II.1); melting point: 205° C.-207° C. (hydrochloride).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07652138B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-7c93c3acf8b644ffa3c634ed5ba2b7cb |
| Source note | uspto-grants-2010_01 |