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HRID1994223

反应详情

EQUATION

反应方程式

HRID 1994223 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)C(O)(c1ccc(C)cc1)c1ccc(C)cc1
HCID22574226

未命名化合物

结构：CN1[C@@H]2CC=C[C@@]1(O)CC2
HCID53629842

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc(C(O)(C(=O)O[C@]23C=CC[C@H](CC2)N3C)c2ccc(C)cc2)cc1
HCID86761046

未命名化合物

PROCEDURE

实验过程

4.10 is prepared analogously to the method according to II.1. Yield: 3.55 g (81% of theory) starting from 2.87 g (0.01 mol) of 3e and 1.48 g (0.01 mol) of tropenol; to purify it, the hydrochloride was precipitated and recrystallized from acetonitrile. Melting point: 232° C.-233° C. (hydrochloride).

WORKUP

后处理

  1. custom4.10 is prepared analogously to the method
  2. customto purify it
  3. customthe hydrochloride was precipitated
  4. customrecrystallized from acetonitrile